VALIDATION OF THE QUANTITATIVE HIGH-PERFORMANCE LIQUID CHROMATOGRAPHY-TANDEM MASS SPECTROMETRY METHOD FOR OKADAIC ACID GROUP TOXINS AND AZASPIRACIDS DETERMINATION IN MOLLUSCS
The quantitative HPLC-MS/MS method for okadaic acid, dinophysis toxins, pectenotoxins, and azaspiracids determination in molluscs was validated using the Commission Decision 657/2002/EC as guideline. Specificity, linearity, reproducibility, trueness, precision, repeatability, decision limits, detection capabilities, and expanded uncertainties in measurements were estimated.